Structure: Comparing NMR and XPS Quantitation I

C1s XPS Spectra

19F NMR Spectra

10/50

HFPO

10/200

HFPO

10/400

HFPO

SJ Limb, DJ Edell, EF Gleason, KK Gleason

J. Appl. Polym. Sci., 67, 1489 (1998)

KKS Lau, KK Gleason

J. Phys. Chem. B, 102, 5977 (1998)

NMR provides more

structural detail

and is more sensitive

to small changes

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